Tris(triorganostannyltetrazoles): Synthesis and supramolecular structures

Michael Hill; Mary F. Mahon; Kieran C. Molloy

doi:10.1039/dt9960001857

Tris(triorganostannyltetrazoles): Synthesis and supramolecular structures

Michael Hill, Mary F. Mahon, Kieran C. Molloy

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Abstract

Six trifunctional triorganotin tetrazoles, (R₃SnN₄CCH₂CH₂)₃C(NO ₂) and 1,3,5-(R₃SnN₄C)₃C₆H₃(R = Me, Et or Bu), have been synthesised by a cycloaddition route from SnR₃(N₃) and either (NCCH₂CH₂)₃C(NO₂) or 1,3,5-(NC)₃C₆H₃ as dipblarophile. The compounds have been characterised by ¹H, ¹³C, ¹¹⁹Sn NMR and ¹¹⁹Mössbauer spectroscopies, while the crystal structures of the tributyltin examples of each series reveal they adopt layered supramolecular arrays.

Original language	English
Pages (from-to)	1857-1865
Number of pages	9
Journal	Journal of the Chemical Society - Dalton Transactions
Issue number	9
DOIs	https://doi.org/10.1039/dt9960001857
Publication status	Published - 7 May 1996

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Chemistry(all)

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title = "Tris(triorganostannyltetrazoles): Synthesis and supramolecular structures",

abstract = "Six trifunctional triorganotin tetrazoles, (R3SnN4CCH2CH2)3C(NO 2) and 1,3,5-(R3SnN4C)3C6H3(R = Me, Et or Bu), have been synthesised by a cycloaddition route from SnR3(N3) and either (NCCH2CH2)3C(NO2) or 1,3,5-(NC)3C6H3 as dipblarophile. The compounds have been characterised by 1H, 13C, 119Sn NMR and 119M{\"o}ssbauer spectroscopies, while the crystal structures of the tributyltin examples of each series reveal they adopt layered supramolecular arrays.",

author = "Michael Hill and Mahon, {Mary F.} and Molloy, {Kieran C.}",

year = "1996",

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T1 - Tris(triorganostannyltetrazoles)

T2 - Synthesis and supramolecular structures

AU - Hill, Michael

AU - Mahon, Mary F.

AU - Molloy, Kieran C.

PY - 1996/5/7

Y1 - 1996/5/7

N2 - Six trifunctional triorganotin tetrazoles, (R3SnN4CCH2CH2)3C(NO 2) and 1,3,5-(R3SnN4C)3C6H3(R = Me, Et or Bu), have been synthesised by a cycloaddition route from SnR3(N3) and either (NCCH2CH2)3C(NO2) or 1,3,5-(NC)3C6H3 as dipblarophile. The compounds have been characterised by 1H, 13C, 119Sn NMR and 119Mössbauer spectroscopies, while the crystal structures of the tributyltin examples of each series reveal they adopt layered supramolecular arrays.

AB - Six trifunctional triorganotin tetrazoles, (R3SnN4CCH2CH2)3C(NO 2) and 1,3,5-(R3SnN4C)3C6H3(R = Me, Et or Bu), have been synthesised by a cycloaddition route from SnR3(N3) and either (NCCH2CH2)3C(NO2) or 1,3,5-(NC)3C6H3 as dipblarophile. The compounds have been characterised by 1H, 13C, 119Sn NMR and 119Mössbauer spectroscopies, while the crystal structures of the tributyltin examples of each series reveal they adopt layered supramolecular arrays.

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JO - Dalton Transactions

JF - Dalton Transactions

SN - 1477-9226

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ER -

Tris(triorganostannyltetrazoles): Synthesis and supramolecular structures

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