The synthesis of deuteriated tri-tert-butyl phosphine

Lucy C. Brown; Anne McGrogan; Yoan Delavoux; James M. Hogg; John D. Holbrey; H. Q. Nimal Gunaratne; Małgorzata Swadźba-Kwaśny; James P. Tellam; Sarah E. Youngs

doi:10.1002/jlcr.4001

The synthesis of deuteriated tri-tert-butyl phosphine

Lucy C. Brown, Anne McGrogan, Yoan Delavoux, James M. Hogg, John D. Holbrey, H. Q. Nimal Gunaratne, Małgorzata Swadźba-Kwaśny, James P. Tellam, Sarah E. Youngs

Research output: Contribution to journal › Article › peer-review

1 Citation (SciVal)

Abstract

The synthesis of deuteriated tri-tert-butyl phosphine is reported. This synthesis is an adaptation of the known procedure for tri-tert-butyl phosphine via a Grignard intermediate.

Original language	English
Pages (from-to)	338-342
Number of pages	5
Journal	Journal of Labelled Compounds and Radiopharmaceuticals
Volume	65
Issue number	13
Early online date	30 Aug 2022
DOIs	https://doi.org/10.1002/jlcr.4001
Publication status	Published - 30 Nov 2022

Keywords

Grignard
perdeuteriated
perdeuteriated ligands
phosphine
phosphine frustrated Lewis pairs
PtBu3
transition metal catalysis
tri-tert-butyl phosphine

ASJC Scopus subject areas

Analytical Chemistry
Biochemistry
Radiology Nuclear Medicine and imaging
Drug Discovery
Spectroscopy
Organic Chemistry

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10.1002/jlcr.4001Licence: CC BY

Cite this

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title = "The synthesis of deuteriated tri-tert-butyl phosphine",

abstract = "The synthesis of deuteriated tri-tert-butyl phosphine is reported. This synthesis is an adaptation of the known procedure for tri-tert-butyl phosphine via a Grignard intermediate.",

keywords = "Grignard, perdeuteriated, perdeuteriated ligands, phosphine, phosphine frustrated Lewis pairs, PtBu3, transition metal catalysis, tri-tert-butyl phosphine",

author = "Brown, {Lucy C.} and Anne McGrogan and Yoan Delavoux and Hogg, {James M.} and Holbrey, {John D.} and Gunaratne, {H. Q. Nimal} and Ma{\l}gorzata Swad{\'z}ba-Kwa{\'s}ny and Tellam, {James P.} and Youngs, {Sarah E.}",

year = "2022",

month = nov,

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doi = "10.1002/jlcr.4001",

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journal = "Journal of Labelled Compounds and Radiopharmaceuticals",

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T1 - The synthesis of deuteriated tri-tert-butyl phosphine

AU - Brown, Lucy C.

AU - McGrogan, Anne

AU - Delavoux, Yoan

AU - Hogg, James M.

AU - Holbrey, John D.

AU - Gunaratne, H. Q. Nimal

AU - Swadźba-Kwaśny, Małgorzata

AU - Tellam, James P.

AU - Youngs, Sarah E.

PY - 2022/11/30

Y1 - 2022/11/30

N2 - The synthesis of deuteriated tri-tert-butyl phosphine is reported. This synthesis is an adaptation of the known procedure for tri-tert-butyl phosphine via a Grignard intermediate.

AB - The synthesis of deuteriated tri-tert-butyl phosphine is reported. This synthesis is an adaptation of the known procedure for tri-tert-butyl phosphine via a Grignard intermediate.

KW - Grignard

KW - perdeuteriated

KW - perdeuteriated ligands

KW - phosphine

KW - phosphine frustrated Lewis pairs

KW - PtBu3

KW - transition metal catalysis

KW - tri-tert-butyl phosphine

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U2 - 10.1002/jlcr.4001

DO - 10.1002/jlcr.4001

M3 - Article

C2 - 36041885

AN - SCOPUS:85137560114

SN - 0362-4803

VL - 65

SP - 338

EP - 342

JO - Journal of Labelled Compounds and Radiopharmaceuticals

JF - Journal of Labelled Compounds and Radiopharmaceuticals

IS - 13

ER -

The synthesis of deuteriated tri-tert-butyl phosphine

Abstract

Keywords

ASJC Scopus subject areas

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Avance 300 MHz Nuclear Magnetic Resonance (NMR) Spectrometer (1South)

Cite this

The synthesis of deuteriated tri-tert-butyl phosphine

Abstract

Keywords

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Equipment

Avance 300 MHz Nuclear Magnetic Resonance (NMR) Spectrometer (1South)

Cite this