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An efficient one-pot ruthenium-catalyzed hydrogen-transfer strategy for a direct access to α,β-unsaturated aldehydes has been developed. The employment of enolates prepared in situ from alcohols avoided handling unstable aldehydes and provided a very appealing route to different cinnamaldehydes substituted in position 2. A silica-grafted amine was used as phase-switch tag leading to a selective one-pot process in favor of cross-dehydrogenative coupling products.
ASJC Scopus subject areas
- Organic Chemistry
- Physical and Theoretical Chemistry
FingerprintDive into the research topics of 'Synthesis of α,β-unsaturated aldehydes based on a one-pot phase-switch dehydrogenative cross-coupling of primary alcohols'. Together they form a unique fingerprint.
- 1 Finished
1/08/11 → 10/05/13
Project: Research council