Synthesis and X-Ray structure analysis of 13,17-bis(2-methoxycarbonylethyl) -12,18-bis(methoxycarbonylmethyl)-2,2,8,8,20-pentamethylisobacteriochlorin

Colin L. Gibson; Michael J. Doyle; Paul R. Raithby; Alan R. Battersby

doi:10.1039/p19940001893

Synthesis and X-Ray structure analysis of 13,17-bis(2-methoxycarbonylethyl) -12,18-bis(methoxycarbonylmethyl)-2,2,8,8,20-pentamethylisobacteriochlorin

Colin L. Gibson, Michael J. Doyle, Paul R. Raithby, Alan R. Battersby

University of Cambridge

Research output: Contribution to journal › Article › peer-review

Abstract

An improved synthesis is developed for the crystalline isobacteriochlorin 5 which carries a 20-methyl group. X-Ray analysis shows that the molecule 5 is substantially puckered in contrast to a close relative lacking the 20-methyl group which is planar.

Original language	English
Pages (from-to)	1893-1895
Number of pages	3
Journal	Journal of the Chemical Society, Perkin Transactions 1
Issue number	14
DOIs	https://doi.org/10.1039/p19940001893
Publication status	Published - 1 Jan 1994

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General Chemistry

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10.1039/p19940001893

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Synthesis and X-Ray structure analysis of 13,17-bis(2-methoxycarbonylethyl) -12,18-bis(methoxycarbonylmethyl)-2,2,8,8,20-pentamethylisobacteriochlorin. / Gibson, Colin L.; Doyle, Michael J.; Raithby, Paul R. et al.
In: Journal of the Chemical Society, Perkin Transactions 1, No. 14, 01.01.1994, p. 1893-1895.

Research output: Contribution to journal › Article › peer-review

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title = "Synthesis and X-Ray structure analysis of 13,17-bis(2-methoxycarbonylethyl) -12,18-bis(methoxycarbonylmethyl)-2,2,8,8,20-pentamethylisobacteriochlorin",

abstract = "An improved synthesis is developed for the crystalline isobacteriochlorin 5 which carries a 20-methyl group. X-Ray analysis shows that the molecule 5 is substantially puckered in contrast to a close relative lacking the 20-methyl group which is planar.",

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Synthesis and X-Ray structure analysis of 13,17-bis(2-methoxycarbonylethyl) -12,18-bis(methoxycarbonylmethyl)-2,2,8,8,20-pentamethylisobacteriochlorin

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