Simple protocol for NMR analysis of the enantiomeric purity of primary amines

Y Perez-Fuertes; A M Kelly; A L Johnson; S Arimori; S D Bull; T D James

doi:10.1021/ol052776g

Simple protocol for NMR analysis of the enantiomeric purity of primary amines

Y Perez-Fuertes
, A M Kelly
, A L Johnson
, S Arimori
, S D Bull
, T D James

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

105 Citations (SciVal)

Abstract

A practically simple three-component chiral derivatizing protocol for determining the enantiopurity of 13 chiral primary amines by H-1 NMR spectroscopic analysis is described, including analysis of those that contain remote stereocenters.

Original language	English
Pages (from-to)	609-612
Number of pages	4
Journal	Organic Letters
Volume	8
Issue number	4
DOIs	https://doi.org/10.1021/ol052776g
Publication status	Published - 2006

Bibliographical note

ID number: ISI:000235534800016

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10.1021/ol052776g

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title = "Simple protocol for NMR analysis of the enantiomeric purity of primary amines",

abstract = "A practically simple three-component chiral derivatizing protocol for determining the enantiopurity of 13 chiral primary amines by H-1 NMR spectroscopic analysis is described, including analysis of those that contain remote stereocenters.",

author = "Y Perez-Fuertes and Kelly, \{A M\} and Johnson, \{A L\} and S Arimori and Bull, \{S D\} and James, \{T D\}",

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journal = "Organic Letters",

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T1 - Simple protocol for NMR analysis of the enantiomeric purity of primary amines

AU - Perez-Fuertes, Y

AU - Kelly, A M

AU - Johnson, A L

AU - Arimori, S

AU - Bull, S D

AU - James, T D

N1 - ID number: ISI:000235534800016

PY - 2006

Y1 - 2006

N2 - A practically simple three-component chiral derivatizing protocol for determining the enantiopurity of 13 chiral primary amines by H-1 NMR spectroscopic analysis is described, including analysis of those that contain remote stereocenters.

AB - A practically simple three-component chiral derivatizing protocol for determining the enantiopurity of 13 chiral primary amines by H-1 NMR spectroscopic analysis is described, including analysis of those that contain remote stereocenters.

U2 - 10.1021/ol052776g

DO - 10.1021/ol052776g

M3 - Article

SN - 1523-7060

VL - 8

SP - 609

EP - 612

JO - Organic Letters

JF - Organic Letters

IS - 4

ER -

Simple protocol for NMR analysis of the enantiomeric purity of primary amines

Abstract

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