One-Pot o-Nitrobenzenesulfonylhydrazide (NBSH) Formation-Diimide Alkene Reduction Protocol

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Abstract

A one-pot protocol for the formation of 2-nitrobenzenesulfo-nylhydrazide (NBSH) from commercial reagents and subsequent alkene reduction is presented. The transformation is operationally simple and generally efficient for effecting diimide alkene reductions. A range of 16 substrates have been reduced, highlighting the unique chemoselectivity of diimide as a reduction system.
Original languageEnglish
Pages (from-to)3186-3188
Number of pages3
JournalJournal of Organic Chemistry
Volume74
Issue number8
DOIs
Publication statusPublished - 17 Apr 2009

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