Microscale Mapping of Fiber Strain and Damage in Composite Wrinkled Laminates Using Computed Tomography Assisted Wide-Angle X-Ray Scattering

Hoang Minh Luong, James Trevarthen, Igor Dolbnya, Wadwan Singhapong, Nicholas Pilato, Richard Butler, Jiraphant Srisuriyachot, Alexander J G Lunt

Research output: Contribution to journalArticlepeer-review

Abstract

Out-of-plane fiber wrinkles in carbon-fiber-reinforced polymer laminates trigger premature failure, yet remain difficult to detect and assess. This study introduces a powerful new diagnostic capability: the pairing of X-ray computed tomography (XCT) and Wide Angle X-ray Scattering (WAXS) during in situ compression of specimens containing small (0.2 mm) and large (0.5 mm) wrinkles. This approach enables, for the first time, detailed field-resolved mapping of axial ((Formula presented.)) and radial ((Formula presented.)) lattice microstrain. A new orientation-aware reduction pipeline supports texture classification, peak fitting, and per-point zero-load referencing, requiring minimal intervention and enabling scalable industrial deployment. In large wrinkles, radial microstrain reached −14.5 µ (Formula presented.) −1, compared to −11.0 µ (Formula presented.) −1 axially; small wrinkles exhibit approximately one-third of this magnitude. Strain hotspots are identified prior to failure, and tomography confirms these regions as the origin of delamination, matrix cracking, and fiber kink banding. To verify the results analytically, a compact, orientation-aware predictor is developed, reproducing measured fields with a mean absolute error on the order of (Formula presented.). These findings establish radial microstrain gradients as a robust, non-destructive indicator of wrinkle severity, providing unique insight and enabling defect behavior to be embedded into full-scale modeling. This supports performance-based rejection criteria and targets inspection in aerospace laminates.

Original languageEnglish
Article number e19053
Number of pages24
JournalAdvanced Science
Early online date3 Dec 2025
DOIs
Publication statusE-pub ahead of print - 3 Dec 2025

Data Availability Statement

The data that support the findings of this study are available from the corresponding author upon reasonable request.

Funding

Dowty Propellers–GE Aviation (United Kingdom) provided the samples which made this study possible. This project was funded by the Science and Technology Facilities Council (STFC) under Diamond Light Source proposal MM31723-1, and by Dowty Propellers-GE Aviation.

FundersFunder number
Science and Technology Facilities Council

Keywords

  • X-ray computed tomography (XCT)
  • carbon fibers reinforced polymer (CFRP) composites
  • lattice strain mapping
  • out-of-plane wrinkles
  • wide angle X-ray scattering (WAXS)

ASJC Scopus subject areas

  • Medicine (miscellaneous)
  • General Chemical Engineering
  • Biochemistry, Genetics and Molecular Biology (miscellaneous)
  • General Materials Science
  • General Engineering
  • General Physics and Astronomy

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