Compact multichannel reactor for liquid phase oxidation of organic feedstocks

D V Bavykin, S T Kolaczkowski, A A Lapkin, P K Plucinski

Research output: Contribution to conferencePaper

Abstract

The design of a multichannel packed bed catalytic reactor to produce chems. for the pharmaceutical and specialty chems. industries is described. This has an integrated heat exchange function, gas/liq. mixing zone, and a reactant injection system. Results are presented for the oxidn. (using gaseous oxygen) of benzyl alc. to benzaldehyde (using toluene as a solvent) over a Ru/Al2O3 catalyst. This system was chosen as a model chem. reaction to study the concept of an integrated multichannel reactor. Results from the catalytic oxidn. expts. showed that the multichannel reactor is suitable for such three-phase catalytic reactions. Conversions up to 25% per 10 cm bed length were measured, giving TOF = 800 h-1, which is close to that reported in the literature for the same catalyst. By controlling the point of injection of oxygen into the reactor an increase in the yield of benzaldehyde formation was achieved. Due to efficient heat transfer the reactor behaved isothermally, despite a 35 Deg adiabatic temp. rise. [on SciFinder (R)]

Conference

ConferenceWorld Congress of Chemical Engineering, 7th
CountryUK United Kingdom
CityGlasgow
Period10/07/0514/07/05

Fingerprint

Feedstocks
Oxidation
Catalysts
Oxygen
Packed beds
Liquids
Drug products
Toluene
Heat transfer
Gases
Industry
Hot Temperature

Keywords

  • compact multichannel reactor for liq. phase oxidn. of org. feedstocks)
  • Reactors (compact multichannel reactor for liq. phase oxidn. of org. feedstocks)
  • Oxidation (catalytic
  • liq oxidn org feedstock multichannel reactor

Cite this

Bavykin, D. V., Kolaczkowski, S. T., Lapkin, A. A., & Plucinski, P. K. (2005). Compact multichannel reactor for liquid phase oxidation of organic feedstocks. Paper presented at World Congress of Chemical Engineering, 7th, Glasgow, UK United Kingdom.

Compact multichannel reactor for liquid phase oxidation of organic feedstocks. / Bavykin, D V; Kolaczkowski, S T; Lapkin, A A; Plucinski, P K.

2005. Paper presented at World Congress of Chemical Engineering, 7th, Glasgow, UK United Kingdom.

Research output: Contribution to conferencePaper

Bavykin, DV, Kolaczkowski, ST, Lapkin, AA & Plucinski, PK 2005, 'Compact multichannel reactor for liquid phase oxidation of organic feedstocks' Paper presented at World Congress of Chemical Engineering, 7th, Glasgow, UK United Kingdom, 10/07/05 - 14/07/05, .
Bavykin DV, Kolaczkowski ST, Lapkin AA, Plucinski PK. Compact multichannel reactor for liquid phase oxidation of organic feedstocks. 2005. Paper presented at World Congress of Chemical Engineering, 7th, Glasgow, UK United Kingdom.
Bavykin, D V ; Kolaczkowski, S T ; Lapkin, A A ; Plucinski, P K. / Compact multichannel reactor for liquid phase oxidation of organic feedstocks. Paper presented at World Congress of Chemical Engineering, 7th, Glasgow, UK United Kingdom.
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AU - Bavykin,D V

AU - Kolaczkowski,S T

AU - Lapkin,A A

AU - Plucinski,P K

PY - 2005

Y1 - 2005

N2 - The design of a multichannel packed bed catalytic reactor to produce chems. for the pharmaceutical and specialty chems. industries is described. This has an integrated heat exchange function, gas/liq. mixing zone, and a reactant injection system. Results are presented for the oxidn. (using gaseous oxygen) of benzyl alc. to benzaldehyde (using toluene as a solvent) over a Ru/Al2O3 catalyst. This system was chosen as a model chem. reaction to study the concept of an integrated multichannel reactor. Results from the catalytic oxidn. expts. showed that the multichannel reactor is suitable for such three-phase catalytic reactions. Conversions up to 25% per 10 cm bed length were measured, giving TOF = 800 h-1, which is close to that reported in the literature for the same catalyst. By controlling the point of injection of oxygen into the reactor an increase in the yield of benzaldehyde formation was achieved. Due to efficient heat transfer the reactor behaved isothermally, despite a 35 Deg adiabatic temp. rise. [on SciFinder (R)]

AB - The design of a multichannel packed bed catalytic reactor to produce chems. for the pharmaceutical and specialty chems. industries is described. This has an integrated heat exchange function, gas/liq. mixing zone, and a reactant injection system. Results are presented for the oxidn. (using gaseous oxygen) of benzyl alc. to benzaldehyde (using toluene as a solvent) over a Ru/Al2O3 catalyst. This system was chosen as a model chem. reaction to study the concept of an integrated multichannel reactor. Results from the catalytic oxidn. expts. showed that the multichannel reactor is suitable for such three-phase catalytic reactions. Conversions up to 25% per 10 cm bed length were measured, giving TOF = 800 h-1, which is close to that reported in the literature for the same catalyst. By controlling the point of injection of oxygen into the reactor an increase in the yield of benzaldehyde formation was achieved. Due to efficient heat transfer the reactor behaved isothermally, despite a 35 Deg adiabatic temp. rise. [on SciFinder (R)]

KW - compact multichannel reactor for liq. phase oxidn. of org. feedstocks)

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KW - Oxidation (catalytic

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