TY - JOUR
T1 - An extremely mild acetate pyrolysis reaction. Novel synthesis and x-ray structure determination of 1-azaspiro[5.5]undecane derivatives
AU - Holmes, Andrew B.
AU - Raithby, Paul R.
AU - Russell, Keith
AU - Stern, Edward S.
AU - Stubbs, Michael E.
AU - Wellard, Nicholas K.
PY - 1984
Y1 - 1984
N2 - The azaspiro oxo-urethane (4), readily available from naphthalene, is reduced to the amino-alcohol (5) whose diacetate (6), the structure of which was determined by X-ray crystallography, undergoes acetate elimination in refluxing toluene to yield the N-acetylazaspiroundecene (7).
AB - The azaspiro oxo-urethane (4), readily available from naphthalene, is reduced to the amino-alcohol (5) whose diacetate (6), the structure of which was determined by X-ray crystallography, undergoes acetate elimination in refluxing toluene to yield the N-acetylazaspiroundecene (7).
UR - http://www.scopus.com/inward/record.url?scp=37049094455&partnerID=8YFLogxK
U2 - 10.1039/c39840001191
DO - 10.1039/c39840001191
M3 - Article
AN - SCOPUS:37049094455
SN - 0022-4936
SP - 1191
EP - 1192
JO - Journal of the Chemical Society, Chemical Communications
JF - Journal of the Chemical Society, Chemical Communications
IS - 17
ER -