A reference high-pressure CH4 adsorption isotherm for zeolite Y: results of an interlaboratory study

H. G.T. Nguyen; C. M. Sims; B. Toman; J. Horn; R. D. van Zee; M. Thommes; R. Ahmad; J. F.M. Denayer; G. V. Baron; E. Napolitano; M. Bielewski; E. Mangano; S. Brandani; D. P. Broom; M. J. Benham; A. Dailly; F. Dreisbach; S. Edubilli; S. Gumma; J. Möllmer; M. Lange; M. Tian; T. J. Mays; T. Shigeoka; S. Yamakita; M. Hakuman; Y. Nakada; K. Nakai; J. Hwang; R. Pini; H. Jiang; A. D. Ebner; M. A. Nicholson; J. A. Ritter; J. Farrando-Pérez; C. Cuadrado-Collados; J. Silvestre-Albero; C. Tampaxis; T. Steriotis; D. Řimnáčová; M. Švábová; M. Vorokhta; H. Wang; E. Bovens; N. Heymans; G. De Weireld

doi:10.1007/s10450-020-00253-0

A reference high-pressure CH₄ adsorption isotherm for zeolite Y: results of an interlaboratory study

H. G.T. Nguyen, C. M. Sims, B. Toman, J. Horn, R. D. van Zee, M. Thommes, R. Ahmad, J. F.M. Denayer, G. V. Baron, E. Napolitano, M. Bielewski, E. Mangano, S. Brandani, D. P. Broom, M. J. Benham, A. Dailly, F. Dreisbach, S. Edubilli, S. Gumma, J. MöllmerM. Lange, M. Tian, T. J. Mays, T. Shigeoka, S. Yamakita, M. Hakuman, Y. Nakada, K. Nakai, J. Hwang, R. Pini, H. Jiang, A. D. Ebner, M. A. Nicholson, J. A. Ritter, J. Farrando-Pérez, C. Cuadrado-Collados, J. Silvestre-Albero, C. Tampaxis, T. Steriotis, D. Řimnáčová, M. Švábová, M. Vorokhta, H. Wang, E. Bovens, N. Heymans, G. De Weireld

Research output: Contribution to journal › Article › peer-review

31 Citations (SciVal)

Abstract

This paper reports the results of an international interlaboratory study led by the National Institute of Standards and Technology (NIST) on the measurement of high-pressure surface excess methane adsorption isotherms on NIST Reference Material RM 8850 (Zeolite Y), at 25 °C up to 7.5 MPa. Twenty laboratories participated in the study and contributed over one-hundred adsorption isotherms of methane on Zeolite Y. From these data, an empirical reference equation was determined, along with a 95% uncertainty interval (U_k=2). By requiring participants to replicate a high-pressure reference isotherm for carbon dioxide adsorption on NIST Reference Material RM 8852 (ZSM-5), this interlaboratory study also demonstrated the usefulness of reference isotherms in evaluating the performance of high-pressure adsorption experiments.

Original language	English
Pages (from-to)	1253-1266
Number of pages	14
Journal	Adsorption
Volume	26
Early online date	11 Sept 2020
DOIs	https://doi.org/10.1007/s10450-020-00253-0
Publication status	Published - 30 Nov 2020

Keywords

CH
CO
High-pressure adsorption isotherm
Interlaboratory study
Reference isotherm
Reference material
RM 8850
RM 8852
Surface excess adsorption
Zeolite Y
ZSM-5

ASJC Scopus subject areas

General Chemistry
General Chemical Engineering
Surfaces and Interfaces

Access to Document

10.1007/s10450-020-00253-0Licence: CC BY

Cite this

Nguyen, H. G. T., Sims, C. M., Toman, B., Horn, J., van Zee, R. D., Thommes, M., Ahmad, R., Denayer, J. F. M., Baron, G. V., Napolitano, E., Bielewski, M., Mangano, E., Brandani, S., Broom, D. P., Benham, M. J., Dailly, A., Dreisbach, F., Edubilli, S., Gumma, S., ... De Weireld, G. (2020). A reference high-pressure CH₄ adsorption isotherm for zeolite Y: results of an interlaboratory study. Adsorption, 26, 1253-1266. https://doi.org/10.1007/s10450-020-00253-0

Nguyen, HGT, Sims, CM, Toman, B, Horn, J, van Zee, RD, Thommes, M, Ahmad, R, Denayer, JFM, Baron, GV, Napolitano, E, Bielewski, M, Mangano, E, Brandani, S, Broom, DP, Benham, MJ, Dailly, A, Dreisbach, F, Edubilli, S, Gumma, S, Möllmer, J, Lange, M, Tian, M, Mays, TJ, Shigeoka, T, Yamakita, S, Hakuman, M, Nakada, Y, Nakai, K, Hwang, J, Pini, R, Jiang, H, Ebner, AD, Nicholson, MA, Ritter, JA, Farrando-Pérez, J, Cuadrado-Collados, C, Silvestre-Albero, J, Tampaxis, C, Steriotis, T, Řimnáčová, D, Švábová, M, Vorokhta, M, Wang, H, Bovens, E, Heymans, N & De Weireld, G 2020, 'A reference high-pressure CH₄ adsorption isotherm for zeolite Y: results of an interlaboratory study', Adsorption, vol. 26, pp. 1253-1266. https://doi.org/10.1007/s10450-020-00253-0

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title = "A reference high-pressure CH4 adsorption isotherm for zeolite Y: results of an interlaboratory study",

abstract = "This paper reports the results of an international interlaboratory study led by the National Institute of Standards and Technology (NIST) on the measurement of high-pressure surface excess methane adsorption isotherms on NIST Reference Material RM 8850 (Zeolite Y), at 25 °C up to 7.5 MPa. Twenty laboratories participated in the study and contributed over one-hundred adsorption isotherms of methane on Zeolite Y. From these data, an empirical reference equation was determined, along with a 95% uncertainty interval (Uk=2). By requiring participants to replicate a high-pressure reference isotherm for carbon dioxide adsorption on NIST Reference Material RM 8852 (ZSM-5), this interlaboratory study also demonstrated the usefulness of reference isotherms in evaluating the performance of high-pressure adsorption experiments.",

keywords = "CH, CO, High-pressure adsorption isotherm, Interlaboratory study, Reference isotherm, Reference material, RM 8850, RM 8852, Surface excess adsorption, Zeolite Y, ZSM-5",

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AU - Nguyen, H. G.T.

AU - Sims, C. M.

AU - Toman, B.

AU - Horn, J.

AU - van Zee, R. D.

AU - Thommes, M.

AU - Ahmad, R.

AU - Denayer, J. F.M.

AU - Baron, G. V.

AU - Napolitano, E.

AU - Bielewski, M.

AU - Mangano, E.

AU - Brandani, S.

AU - Broom, D. P.

AU - Benham, M. J.

AU - Dailly, A.

AU - Dreisbach, F.

AU - Edubilli, S.

AU - Gumma, S.

AU - Möllmer, J.

AU - Lange, M.

AU - Tian, M.

AU - Mays, T. J.

AU - Shigeoka, T.

AU - Yamakita, S.

AU - Hakuman, M.

AU - Nakada, Y.

AU - Nakai, K.

AU - Hwang, J.

AU - Pini, R.

AU - Jiang, H.

AU - Ebner, A. D.

AU - Nicholson, M. A.

AU - Ritter, J. A.

AU - Farrando-Pérez, J.

AU - Cuadrado-Collados, C.

AU - Silvestre-Albero, J.

AU - Tampaxis, C.

AU - Steriotis, T.

AU - Řimnáčová, D.

AU - Švábová, M.

AU - Vorokhta, M.

AU - Wang, H.

AU - Bovens, E.

AU - Heymans, N.

AU - De Weireld, G.

PY - 2020/11/30

Y1 - 2020/11/30

N2 - This paper reports the results of an international interlaboratory study led by the National Institute of Standards and Technology (NIST) on the measurement of high-pressure surface excess methane adsorption isotherms on NIST Reference Material RM 8850 (Zeolite Y), at 25 °C up to 7.5 MPa. Twenty laboratories participated in the study and contributed over one-hundred adsorption isotherms of methane on Zeolite Y. From these data, an empirical reference equation was determined, along with a 95% uncertainty interval (Uk=2). By requiring participants to replicate a high-pressure reference isotherm for carbon dioxide adsorption on NIST Reference Material RM 8852 (ZSM-5), this interlaboratory study also demonstrated the usefulness of reference isotherms in evaluating the performance of high-pressure adsorption experiments.

AB - This paper reports the results of an international interlaboratory study led by the National Institute of Standards and Technology (NIST) on the measurement of high-pressure surface excess methane adsorption isotherms on NIST Reference Material RM 8850 (Zeolite Y), at 25 °C up to 7.5 MPa. Twenty laboratories participated in the study and contributed over one-hundred adsorption isotherms of methane on Zeolite Y. From these data, an empirical reference equation was determined, along with a 95% uncertainty interval (Uk=2). By requiring participants to replicate a high-pressure reference isotherm for carbon dioxide adsorption on NIST Reference Material RM 8852 (ZSM-5), this interlaboratory study also demonstrated the usefulness of reference isotherms in evaluating the performance of high-pressure adsorption experiments.

KW - CH

KW - CO

KW - High-pressure adsorption isotherm

KW - Interlaboratory study

KW - Reference isotherm

KW - Reference material

KW - RM 8850

KW - RM 8852

KW - Surface excess adsorption

KW - Zeolite Y

KW - ZSM-5

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U2 - 10.1007/s10450-020-00253-0

DO - 10.1007/s10450-020-00253-0

M3 - Article

AN - SCOPUS:85090499362

SN - 0929-5607

VL - 26

SP - 1253

EP - 1266

JO - Adsorption

JF - Adsorption

ER -