A new polymorph of [(S)-(-)-2-aminomethyl-1-ethylpyrrolidine-kappa N-2,N '](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate

M D Jones; F A A Paz; J E Davies; B F G Johnson; J Klinowski

doi:10.1107/s1600536803024760

A new polymorph of [(S)-(-)-2-aminomethyl-1-ethylpyrrolidine-kappa N-2,N '](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate

M D Jones, F A A Paz, J E Davies, B F G Johnson, J Klinowski

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

2 Citations (SciVal)

Abstract

The structure of a new polymorph of the title compound, [Rh(C8H12)(C7H16N2)]CF3SO3, the first form of which we recently reported [Rouzaud et al. (2003). Helv. Chim. Acta, 86, 1753-1759], has been determined at 180 K in space group C222(1). The differences between the two polymorphs, are related to the way the individual ions close-pack within the unit cell.

Original language	English
Pages (from-to)	M1091-M1093
Journal	Acta Crystallographica Section E-Structure Reports Online
Volume	59
DOIs	https://doi.org/10.1107/s1600536803024760
Publication status	Published - 2003

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ID number: ISI:000186886200007

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title = "A new polymorph of [(S)-(-)-2-aminomethyl-1-ethylpyrrolidine-kappa N-2,N '](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate",

abstract = "The structure of a new polymorph of the title compound, [Rh(C8H12)(C7H16N2)]CF3SO3, the first form of which we recently reported [Rouzaud et al. (2003). Helv. Chim. Acta, 86, 1753-1759], has been determined at 180 K in space group C222(1). The differences between the two polymorphs, are related to the way the individual ions close-pack within the unit cell.",

author = "Jones, {M D} and Paz, {F A A} and Davies, {J E} and Johnson, {B F G} and J Klinowski",

note = "ID number: ISI:000186886200007",

year = "2003",

doi = "10.1107/s1600536803024760",

language = "English",

volume = "59",

pages = "M1091--M1093",

journal = "Acta Crystallographica Section E-Structure Reports Online",

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publisher = "International Union of Crystallography",

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TY - JOUR

T1 - A new polymorph of [(S)-(-)-2-aminomethyl-1-ethylpyrrolidine-kappa N-2,N '](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate

AU - Jones, M D

AU - Paz, F A A

AU - Davies, J E

AU - Johnson, B F G

AU - Klinowski, J

N1 - ID number: ISI:000186886200007

PY - 2003

Y1 - 2003

N2 - The structure of a new polymorph of the title compound, [Rh(C8H12)(C7H16N2)]CF3SO3, the first form of which we recently reported [Rouzaud et al. (2003). Helv. Chim. Acta, 86, 1753-1759], has been determined at 180 K in space group C222(1). The differences between the two polymorphs, are related to the way the individual ions close-pack within the unit cell.

AB - The structure of a new polymorph of the title compound, [Rh(C8H12)(C7H16N2)]CF3SO3, the first form of which we recently reported [Rouzaud et al. (2003). Helv. Chim. Acta, 86, 1753-1759], has been determined at 180 K in space group C222(1). The differences between the two polymorphs, are related to the way the individual ions close-pack within the unit cell.

U2 - 10.1107/s1600536803024760

DO - 10.1107/s1600536803024760

M3 - Article

SN - 1600-5368

VL - 59

SP - M1091-M1093

JO - Acta Crystallographica Section E-Structure Reports Online

JF - Acta Crystallographica Section E-Structure Reports Online

ER -

A new polymorph of [(S)-(-)-2-aminomethyl-1-ethylpyrrolidine-kappa N-2,N '](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate

Abstract

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