A New Method for the Synthesis of Heterometallic Complexes: Syntheses and Structures of [(PhCH2CH2NLi)3Sb(thf)]2 and [Sb3(cyN)4(NMe2)2]Li

Andrew J. Edwards, Michael A. Paver, Paul R. Raithby, Moira‐Ann ‐A Rennie, Christopher A. Russell, Dominic S. Wright

Research output: Contribution to journalArticlepeer-review

Abstract

Successive metalation of primary amines, first with nBuLi and then with Sb(NMe2)3, has enabled the preparation of the heterometallic complexes 1 and 2. Neutra [Ph(CH2)2N(H)Li]n and ionic Li[Sb(cyNH)4] occur as the intermediates in the formation of 1 and 2, respectively. (Formula Presented.)

Original languageEnglish
Pages (from-to)1277-1279
Number of pages3
JournalAngewandte Chemie International Edition in English
Volume33
Issue number12
DOIs
Publication statusPublished - 6 Jun 1994

ASJC Scopus subject areas

  • Catalysis
  • General Chemistry

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