A new approach for obtaining ceramic NASICON (Na3Zr2Si2PO12) films sintered in situ by a sol-gel method, using spray deposition and near-infra red sintering

Rafael Marti Valls; Rebecca Griffin; Anne Sawhney; Celina Domingos-Dlofo; Tom Dunlop; Sam Reis; Peter J. Holliman; Jenny Baker

doi:10.1039/d4ta05747c

A new approach for obtaining ceramic NASICON (Na₃Zr₂Si₂PO₁₂) films sintered in situ by a sol-gel method, using spray deposition and near-infra red sintering

Rafael Marti Valls
, Rebecca Griffin
, Anne Sawhney
, Celina Domingos-Dlofo
, Tom Dunlop
, Sam Reis
, Peter J. Holliman
, Jenny Baker

Swansea University

Research output: Contribution to journal › Article › peer-review

1 Citation (SciVal)

Abstract

In this work we demonstrate a NASICON film sintered in situ onto a fused silica substrate. This production method drastically reduces the manufacturing time by combining the use of a spray-coated sol-gel solution and near-infrared (NIR) ultrafast sintering technology. This is the first demonstration of NIR sintered ceramics at high temperatures (∼1000 °C).

Original language	English
Pages (from-to)	31116-31120
Number of pages	5
Journal	Journal of Materials Chemistry A
Volume	12
Issue number	45
Early online date	29 Oct 2024
DOIs	https://doi.org/10.1039/d4ta05747c
Publication status	Published - 7 Dec 2024

Data Availability Statement

The data supporting this article have been included as part of the ESI.†

Funding

We gratefully acknowledge funding from the EPSRC ECR Fellowship NoRESt EP/S03711X/1 (JB, RMV, AS, BG,and CD-D), EPSRC/Tata Steel for co-sponsoring an iCASE PhD studentship (Grant number: 2610332) (Voucher # 20000176) for SR and the Sustain Hub (EP/S018107/1) for PJH and HEFCW for the funding capital grant for the STA. The authors would like to acknowledge the access to characterisation equipment at the Swansea University Advanced Imaging of Materials (AIM) facility, which was funded in part by the EPSRC (EP/M028267/1) and the European Regional Development Fund through the Welsh Government (80708). This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

SDG 7 Affordable and Clean Energy

ASJC Scopus subject areas

General Chemistry
Renewable Energy, Sustainability and the Environment
General Materials Science

Access to Document

10.1039/d4ta05747cLicence: CC BY

Cite this

A new approach for obtaining ceramic NASICON (Na₃Zr₂Si₂PO₁₂) films sintered in situ by a sol-gel method, using spray deposition and near-infra red sintering. / Valls, Rafael Marti; Griffin, Rebecca; Sawhney, Anne et al.
In: Journal of Materials Chemistry A, Vol. 12, No. 45, 07.12.2024, p. 31116-31120.

Research output: Contribution to journal › Article › peer-review

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