Dataset for 'PrFeO3 photocathodes prepared through spray pyrolysis'

PrFeO3 (PFO) has been shown to be an active photochemical water reduction in slurry reactors, but has yet to be shown as a photocathode for photoelectrochemical water reduction, to the best of our knowledge. The work herein describes the fabrication of active PFO photocathodes through a spray pyrolysis method with subsequent calcination at 500, 600 and 700˚C. The films were prepared on fluorine-doped tin oxide aluminoborosilcate glass for the application of solar water reduction. This dataset includes characterisation of these PFO films including, XRD, XPS, photoelectrochemical measurements and electronic impedance spectroscopy measurements. Datasets are also included from those incorporated within the supplementary information.